benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name)
benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name)
CAS: 10065-79-9
Molecular Formula: C17H17N3O4
benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name) - Names and Identifiers
| Name | benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name) |
| Synonyms | Nsc293361 N,N'-Bis-CBZ-guanidine N,N'-Bis(benzyloxycarbonyl)guanidine benzyl N-(N-phenylmethoxycarbonylcarbamimidoyl)carbamate benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbama... benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name) (NZ)-N-[amino(phenylmethoxycarbonylamino)methylidene]carbamic acid (phenylmethyl) ester |
| CAS | 10065-79-9 |
| InChI | InChI=1/C17H17N3O4/c18-15(19-16(21)23-11-13-7-3-1-4-8-13)20-17(22)24-12-14-9-5-2-6-10-14/h1-10H,11-12H2,(H3,18,19,20,21,22) |
benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name) - Physico-chemical Properties
| Molecular Formula | C17H17N3O4 |
| Molar Mass | 327.338 |
| Density | 1.24g/cm3 |
| Storage Condition | under inert gas (nitrogen or Argon) at 2–8 °C |
| Refractive Index | 1.586 |
benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name) - Introduction
N,N-bis (benzyloxycarbonyl) guanidine, also known as DBN, is an organic compound. The following is a description of its nature, use, preparation and safety information:
Nature:
N,N-bis (benzyloxycarbonyl) guanidine is a colorless to pale yellow crystal, soluble in some organic solvents such as ethanol, acetone and dichloromethane, insoluble in water. It has high thermal stability and low toxicity.
Use:
N,N-bis (benzyloxycarbonyl) guanidine is mainly used as a weak base catalyst in organic synthesis. It is commonly used in a variety of reactions, including esterification, acylation, condensation, and nucleophilic substitution. It can also be used as an acid scavenger, ligand and dehydrating agent for hydroxides.
Preparation Method:
N,N-bis (benzyloxycarbonyl) guanidine can be prepared by reacting benzylamine with dimethylformamide. First, benzylamine and dimethylformamide were placed in a reaction flask, and the reaction was stirred at room temperature for a period of time. Subsequently, the resulting mixture is subjected to crystallization or rotary evaporation to obtain N,N-bis (benzyloxycarbonyl) guanidine.
Safety Information:
N,N-bis (benzyloxycarbonyl) guanidine is relatively safe under normal conditions of use, but the following matters still need to be noted:
1. Use appropriate personal protective equipment, such as lab gloves, goggles and lab clothes.
2. avoid inhaling its dust and gas. It should be operated in a well-ventilated place to prevent its vapor accumulation.
3. Avoid contact with strong oxidants and acidic substances to avoid dangerous reactions.
4. storage should be sealed, away from the fire and flammable materials.
Nature:
N,N-bis (benzyloxycarbonyl) guanidine is a colorless to pale yellow crystal, soluble in some organic solvents such as ethanol, acetone and dichloromethane, insoluble in water. It has high thermal stability and low toxicity.
Use:
N,N-bis (benzyloxycarbonyl) guanidine is mainly used as a weak base catalyst in organic synthesis. It is commonly used in a variety of reactions, including esterification, acylation, condensation, and nucleophilic substitution. It can also be used as an acid scavenger, ligand and dehydrating agent for hydroxides.
Preparation Method:
N,N-bis (benzyloxycarbonyl) guanidine can be prepared by reacting benzylamine with dimethylformamide. First, benzylamine and dimethylformamide were placed in a reaction flask, and the reaction was stirred at room temperature for a period of time. Subsequently, the resulting mixture is subjected to crystallization or rotary evaporation to obtain N,N-bis (benzyloxycarbonyl) guanidine.
Safety Information:
N,N-bis (benzyloxycarbonyl) guanidine is relatively safe under normal conditions of use, but the following matters still need to be noted:
1. Use appropriate personal protective equipment, such as lab gloves, goggles and lab clothes.
2. avoid inhaling its dust and gas. It should be operated in a well-ventilated place to prevent its vapor accumulation.
3. Avoid contact with strong oxidants and acidic substances to avoid dangerous reactions.
4. storage should be sealed, away from the fire and flammable materials.
Last Update：2024-04-09 21:01:54
![benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name)](http://res.chembk.com/assets/str/2d/1/10/10065-79-9.png)
Supplier List
Spot supply
Product Name: benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name) Request for quotationCAS: 10065-79-9
Tel: +86-17551318830
Email: r@reformchem.com
Mobile: +86-17551318830
QQ: 3785839865
Product Name: Nsc293361 Visit Supplier Webpage Request for quotation
CAS: 10065-79-9
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
CAS: 10065-79-9
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
Spot supply
Product Name: benzyl (amino{[(benzyloxy)carbonyl]amino}methylidene)carbamate (non-preferred name) Request for quotationCAS: 10065-79-9
Tel: +86-17551318830
Email: r@reformchem.com
Mobile: +86-17551318830
QQ: 3785839865
Product Name: Nsc293361 Visit Supplier Webpage Request for quotation
CAS: 10065-79-9
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
CAS: 10065-79-9
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
View History